Publications

2004

Journal Article

Rudloff, J.; Cölfen, H.: Superstructures of temporarily stabilized nanocrystalline CaCO₃ particles: morphological control via water surface tension variation. Langmuir 20 (3), pp. 991 - 996 (2004)

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Rühe, J.; Ballauff, M.; Biesalski, M.; Dziezok, P.; Gröhn, F.; Johannsmann, D.; Houbenov, N.; Hugenberg, N.; Konradi, R.; Minko, S. et al.; Motornov, M.; Netz, R. R.; Schmidt, M.; Seidel, C.; Stamm, M.; Stephan, T.; Usov, D.; Zhang, H. N.: Polyelectrolyte brushes. Advances in Polymer Science 165, pp. 79 - 150 (2004)

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Ruland, W.; Smarsly, B.: SAXS of self-assembled oriented lamellar nanocomposite film: an advanced method of evaluation. Journal of Applied Crystallography 37, pp. 575 - 584 (2004)

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Schlaad, H.; Krasia, T.; Antonietti, M.: Superhelices of poly[2-(acetoacetoxy)ethyl methacrylate]. Journal of the American Chemical Society 126 (36), pp. 11307 - 11310 (2004)

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Schlaad, H.; Smarsly, B.; Losik, M.: The role of chain-length distribution in the formation of solid-state structures of polypeptide-based rod-coil block copolymers. Macromolecules 37 (6), pp. 2210 - 2214 (2004)

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Sedlak, M.; Tauer, K.: One-step synthesis of new anionic gemini surface active azoinitiators. Synlett (2), pp. 299 - 300 (2004)

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Shchukin, D. G.; Caruso, R. A.: Template synthesis and photocatalytic properties of porous metal oxide spheres formed by nanoparticle infiltration. Chemistry of Materials 16 (11), pp. 2287 - 2292 (2004)

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Sinn, C. G.; Dimova, R.; Antonietti, M.: Isothermal titration calorimetry of the polyelectrolyte/water interaction and binding of Ca²⁺: effects determining the quality of polymeric scale inhibitors. Macromolecules 37 (9), pp. 3444 - 3450 (2004)

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Smarsly, B.; Grosso, D.; Brezesinski, T.; Pinna, N.; Boissiere, C.; Antonietti, M.; Sanchez, C.: Highly crystalline cubic mesoporous TiO₂ with 10-nm pore diameter made with a new block copolymer template. Chemistry of Materials 16 (15), pp. 2948 - 2952 (2004)

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Smarsly, B.; Kuang, D. B.; Antonietti, M.: Making nanometer thick silica glass scaffolds: an experimental approach to learn about size effects in glasses. Colloid and Polymer Science 282 (8), pp. 892 - 900 (2004)

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Taden, A.; Antonietti, M.; Heilig, A.; Landfester, K.: Inorganic films from three different phosphors via a liquid coating route from inverse miniemulsions. Chemistry of Materials 16 (24), pp. 5081 - 5087 (2004)

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Taden, A.; Landfester, K.; Antonietti, M.: Crystallization of dyes by directed aggregation of colloidal intermediates: a model case. Langmuir 20 (3), pp. 957 - 961 (2004)

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Tao, X.; Li, J. B.; Hartmann, J.; Möhwald, H.: Self-assembly and properties of phthalocyanine and polyelectrolytes onto melamine resin particles. New Journal of Chemistry 28 (12), pp. 1579 - 1583 (2004)

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Tauer, K.; Öz, N.: Interfacial energy promotes radical heterophase polymerization. Macromolecules 37 (16), pp. 5880 - 5888 (2004)

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Thünemann, A. F.; Müller, M.; Dautzenberg, H.; Joanny, J. F. O.; Lowne, H.: Polyelectrolyte complexes. Advances in Polymer Science 166, pp. 113 - 171 (2004)

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Tsavalas, J. G.; Schork, F. J.; Landfester, K.: Particle morphology development in hybrid miniemulsion polymerization. JCT Research 1 (1), pp. 53 - 63 (2004)

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Yakubov, G. E.; Loppinet, B.; Zhang, H.; Ruhe, J.; Sigel, R.; Fytas, G.: Collective dynamics of an end-grafted polymer brush in solvents of varying quality. Physical Review Letters 92 (11), 115501 (2004)

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Yu, S. H.; Cölfen, H.: Bio-inspired crystal morphogenesis by hydrophilic polymers. Journal of Materials Chemistry 14 (14), pp. 2124 - 2147 (2004)

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Yu, S. H.; Cölfen, H.; Fischer, A.: High quality CeO₂ nanocrystals stabilized by a double hydrophilic block copolymer. Colloids and Surfaces A: Physicochemical and Engineering Aspects 243 (1-3), pp. 49 - 52 (2004)

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Yu, S. H.; Cölfen, H.; Mastai, Y.: Formation and optical properties of gold nanoparticles synthesized in the presence of double-hydrophilic block copolymers. Journal of Nanoscience and Nanotechnology 4 (3), pp. 291 - 298 (2004)

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Yu, S. H.; Cölfen, H.; Xu, A. W.; Dong, W. F.: Complex spherical BaCO₃ superstructures self-assembled by a facile mineralization process under control of simple polyelectrolytes. Crystal Growth & Design 4 (1), pp. 33 - 37 (2004)

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Yu, S. H.; Cui, X. J.; Li, L. L.; Li, K.; Yu, B.; Antonietti, M.; Cölfen, H.: From starch to metal/carbon hybrid nanostructures: hydrothermal metal-catalyzed carbonization. Advanced Materials 16 (18), pp. 1636 - 1640 (2004)

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Zakrevskyy, Y.; Faul, C. F. J.; Guan, Y.; Stumpe, J.: Alignment of a perylene-based ionic self-assembly complex in thermotropic and lyotropic liquid-crystalline phases. Advanced Functional Materials 14 (9), pp. 835 - 841 (2004)

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Zhou, Y.; Antonietti, M.: A series of highly ordered, super-microporus, lamellar silicas prepared by nanocasting with ionic liquids. Chemistry of Materials 16 (3), pp. 544 - 550 (2004)

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Zhou, Y.; Schattka, J. H.; Antonietti, M.: Room-temperature ionic liquids as template to monolithic mesoporous silica with wormlike pores via a sol-gel nanocasting technique. Nano Letters 4 (3), pp. 477 - 481 (2004)

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2003

Journal Article

Ahmad, H.; Tauer, K.: Effects of chain transfer agent on the radical polymerization of styrene in non-aqueous dispersion. Colloid and Polymer Science 281 (7), pp. 686 - 689 (2003)

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Ahmad, H.; Tauer, K.: Production of micron-sized polystyrene particles containing PEG near the particles surface. Colloid and Polymer Science 281 (5), pp. 476 - 484 (2003)

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Ahmad, H.; Tauer, K.: Poly(ethylene glycol)-coated monodisperse micron-sized composite polymer particles. Macromolecules 36 (3), pp. 648 - 653 (2003)

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Antonietti, M.: Nanostructured materials - Self-organization of functional polymers. Nature Materials 2 (1), pp. 9 - 10 (2003)

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Antonietti, M.; Förster, S.: Vesicles and liposomes: a self-assembly principle beyond lipids. Advanced Materials 15 (16), pp. 1323 - 1333 (2003)

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Antonietti, M.; Tauer, K.: 90 years of polymer latexes and heterophase polymerization: more vital than ever. Macromolecular Chemistry and Physics 204 (2), pp. 207 - 219 (2003)

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Aslamazova, T.; Tauer, K.: On the colloidal stability of polystyrene particles prepared with surface-active initiators. Advances in Colloid and Interface Science 104, pp. 273 - 283 (2003)

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Barrère, M.; Landfester, K.: High molecular weight polyurethane and polymer hybrid particles in aqueous miniemulsion. Macromolecules 36 (14), pp. 5119 - 5125 (2003)

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Barrère, M.; Landfester, K.: Polyester synthesis in aqueous miniemulsion. Polymer 44 (10), pp. 2833 - 2841 (2003)

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Journal Article

Bronstein, L. M.; Chernyshov, D. M.; Karlinsey, R.; Zwanziger, J. W.; Matveeva, V. G.; Sulman, E. M.; Demidenko, G. N.; Hentze, H. P.; Antonietti, M.: Mesoporous alumina and aluminosilica with Pd and Pt nanoparticles: structure and catalytic properties. Chemistry of Materials 15 (13), pp. 2623 - 2631 (2003)

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Budhlall, B. M.; Landfester, K.; Sudol, E. D.; Dimonie, V. L.; Klein, A.; El-Aasser, M. S.: Characterization of partially hydrolyzed poly(vinyl alcohol). Effect of poly(vinyl alcohol) molecular architecture on aqueous phase conformation. Macromolecules 36 (25), pp. 9477 - 9484 (2003)

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Journal Article

Camerel, F.; Antonietti, M.; Faul, C. F. J.: Organized nanostructured complexes of inorganic clusters and surfactants that exhibit thermal solid-state transformations. Chemistry – A European Journal 9 (10), pp. 2160 - 2166 (2003)

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Camerel, F.; Faul, C. F. J.: Combination of ionic self-assembly and hydrogen bonding as a tool for the synthesis of liquid-crystalline materials and organogelators from a simple building block. Chemical Communications (15), pp. 1958 - 1959 (2003)

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Camerel, F.; Strauch, P.; Antonietti, M.; Faul, C. F. J.: Copper-metallomesogen structures obtained by ionic self-assembly (ISA): molecular electromechanical switching driven by cooperativity. Chemistry – A European Journal 9 (16), pp. 3764 - 3771 (2003)

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Journal Article

Cölfen, H.: Precipitation of carbonates: recent progress in controlled production of complex shapes. Current Opinion in Colloid & Interface Science 8 (1), pp. 23 - 31 (2003)

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Journal Article

Cölfen, H.; Mann, S.: Higher-order organization by mesoscale self-assembly and transformation of hybrid nanostructures. Angewandte Chemie International Edition 42 (21), pp. 2350 - 2365 (2003)

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Journal Article

Cölfen, H.; Tirosh, S.; Zaban, A.: Nanocrystal surface structure analysis by analytical ultracentrifugation. Langmuir 19 (26), pp. 10654 - 10659 (2003)

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Cölfen, H.; Völkel, A.: Hybrid colloid analysis combining analytical ultracentrifugation and flow-field flow fractionation. European Biophysics Journal with Biophysics Letters 32 (5), pp. 432 - 436 (2003)

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Journal Article

Dautzenberg, H.; Konak, C.; Reschel, T.; Zintchenko, A.; Ulbrich, K.: Cationic graft copolymers as carriers for delivery of antisense-oligonucleotides. Macromolecular Bioscience 3 (8), pp. 425 - 435 (2003)

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Journal Article

Dautzenberg, H.; Kriz, J.: Response of polyelectrolyte complexes to subsequent addition of salts with different cations. Langmuir 19 (13), pp. 5204 - 5211 (2003)

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Journal Article

Dimitrov, I.; Schlaad, H.: Synthesis of nearly monodisperse polystyrene-polypeptide block copolymers via polymerisation of N-carboxyanhydrides. Chemical Communications (23), pp. 2944 - 2945 (2003)

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Journal Article

Dimova, R.; Lipowsky, R.; Mastai, Y.; Antonietti, M.: Binding of polymers to calcite crystals in water: characterization by isothermal titration calorimetry. Langmuir 19 (15), pp. 6097 - 6103 (2003)

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Journal Article

Endo, H.; Cölfen, H.; Schwahn, D.: An analysis of a polymer additive for calcium carbonate crystallization - a small-angle neutron scattering investigation by applying contrast variation. Journal of Applied Crystallography 36, pp. 568 - 572 (2003)

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Faul, C. F. J.; Antonietti, M.: Ionic self-assembly: facile synthesis of supramolecular materials. Advanced Materials 15 (9), pp. 673 - 683 (2003)

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Journal Article

Faul, C. F. J.; Antonietti, M.; Hentze, H.-P.; Smarsly, B.: Solid-state nanostructure of PAMAM dendrimer-fluorosurfactant complexes and nanoparticles synthesis within the ionic subphase. Colloids and Surfaces A: Physicochemical and Engineering Aspects 212 (2-3), pp. 115 - 121 (2003)

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Journal Article

Ganeva, D.; Antonietti, M.; Faul, C. F. J.; Sanderson, R.: Polymerization of the organized phases of polyelectrolyte-surfactant complexes. Langmuir 19 (16), pp. 6561 - 6565 (2003)

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Ganeva, D.; Faul, C. F. J.; Gotz, C.; Sanderson, R. D.: Directed reactions within confined reaction environments: polyadditions in polyelectrolyte-surfactant complexes. Macromolecules 36 (8), pp. 2862 - 2866 (2003)

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Gernandt, R.; Wagberg, L.; Gardlund, L.; Dautzenberg, H.: Polyelectrolyte complexes for surface modification of wood fibres - I. Preparation and characterisation of complexes for dry and wet strength improvement of paper. Colloids and Surfaces A: Physicochemical and Engineering Aspects 213 (1), pp. 15 - 25 (2003)

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Glinel, K.; Sukhorukov, G. B.; Möhwald, H.; Khrenov, V.; Tauer, K.: Thermosensitive hollow capsules based on thermoresponsive polyelectrolytes. Macromolecular Chemistry and Physics 204 (14), pp. 1784 - 1790 (2003)

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Journal Article

Granick, S.; Kumar, S. K.; Amis, E. J.; Antonietti, M.; Balazs, A. C.; Chakraborty, A. K.; Grest, G. S.; Hawker, C.; Janmey, P.; Kramer, E. J. et al.; Nuzzo, R.; Russell, T. P.; Safinya, C. R.: Macromolecules at surfaces: research challenges and opportunities from tribology to biology. Journal of Polymer Science Part B-Polymer Physics 41 (22), pp. 2755 - 2793 (2003)

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Guan, Y.; Zakrevskyy, Y.; Stumpe, J.; Antonietti, M.; Faul, C. F. J.: Perylenediimide-surfactant complexes: thermotropic liquid- crystalline materials via ionic self-assembly. Chemical Communications (7), pp. 894 - 895 (2003)

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Guo, X.; Condra, M.; Kimura, K.; Berth, G.; Dautzenberg, H.; Dubin, P. L.: Determination of molecular weight of heparin by size exclusion chromatography with universal calibration. Analytical Biochemistry 312 (1), pp. 33 - 39 (2003)

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Journal Article

Han, B. H.; Antonietti, M.: One-step synthesis of copper nanoparticles containing mesoporous silica by nanocasting of binuclear copper(II) complexes with cyclodextrins. Journal of Materials Chemistry 13 (7), pp. 1793 - 1796 (2003)

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Han, B. H.; Smarsly, B.; Gruber, C.; Wenz, G.: Towards porous silica materials via nanocasting of stable pseudopolyrotaxanes from alpha-cyclodextrin and polyamines. Microporous and Mesoporous Materials 66 (1), pp. 127 - 132 (2003)

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Holmqvist, P.; Pispas, S.; Hadjichristidis, N.; Fytas, G.; Sigel, R.: Dynamic structure factor of diblock copolymers solutions in the disordered state. 3. The non-mean-field regime. Macromolecules 36, pp. 830 - 838 (2003)

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Journal Article

Hornebecq, V.; Antonietti, M.; Cardinal, T.; Treguer-Delapierre, M.: Stable silver nanoparticles immobilized in mesoporous silica. Journal of Materials Chemistry 15 (10), pp. 1993 - 1999 (2003)

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Hornebecq, V.; Mastai, Y.; Antonietti, M.; Polarz, S.: Redox behavior of nanostructured molybdenum oxide–Mesoporous silica hybrid materials. Chemistry of Materials 15 (19), pp. 3586 - 3593 (2003)

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Kasatkin, I.; Girgsdies, F.; Ressler, T.; Caruso, R. A.; Schattka, J. H.; Urban, J.; Weiss, K.: HRTEM study of Cu/ZrO₂ catalyst. An evidence of a new perovskite-like oxide ZrCuO₃. Journal of Materials Science Letters 22 (5), pp. 335 - 337 (2003)

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Kietzke, T.; Neher, D.; Landfester, K.; Montenegro, R.; Güntner, R.; Scherf, U.: Novel approaches to polymer blends based on polymer nanoparticles. Nature Materials 2 (6), pp. 408 - 412 (2003)

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Krasia, T.; Soula, R.; Börner, H. G.; Schlaad, H.: Controlled synthesis of homopolymers and block copolymers based on 2-(acetoacetoxy)ethyl methacrylate via RAFT radical polymerisation. Chemical Communications (4), pp. 538 - 539 (2003)

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Landfester, K.; Ramirez, L. P.: Encapsulated magnetite particles for biomedical application. Journal of Physics: Condensed Matter 15 (15), pp. S1345 - S1361 (2003)

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Landfester, K.; Schork, F. J.; Kusuma, V. A.: Particle size distribution in mini-emulsion polymerization. Comptes Rendus Chimie 6, pp. 1337 - 1342 (2003)

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Lohmeijer, B. G. G.; Schlaad, H.; Schubert, U. S.: Synthesis and thermal properties of diblock copolymers utilizing non-covalent interactions. Macromolecular Symposia 196, pp. 125 - 135 (2003)

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Marie, E.; Rothe, R.; Antonietti, M.; Landfester, K.: Synthesis of polyaniline particles via inverse and direct miniemulsion. Macromolecules 36 (11), pp. 3967 - 3973 (2003)

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Montenegro, R.; Antonietti, M.; Mastai, Y.; Landfester, K.: Crystallization in miniemulsion droplets. The Journal of Physical Chemistry B 107 (21), pp. 5088 - 5094 (2003)

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Montenegro, R.; Landfester, K.: Metastable and stable morphologies during crystallization of alkanes in miniemulsion droplets. Langmuir 19 (15), pp. 5996 - 6003 (2003)

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Nordskog, A.; Egger, H.; Findenegg, G. H.; Hellweg, T.; Schlaad, H.; Berlepsch, H. v.; Böttcher, C.: Structural changes of poly(butadiene)-poly(ethyleneoxide) diblock-copolymer micelles induced by a cationic surfactant: scattering and cryogenic transmission electron microscopy studies. Physical Review E 68 (1), 011406 (2003)

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Piok, T.; Gamerith, S.; Gadermaier, C.; Plank, H.; Wenzl, F. P.; Patil, S.; Montenegro, R.; Kietzke, T.; Neher, D.; Scherf, U. et al.; Landfester, K.; List, E. J. W.: Organic light-emitting devices fabricated from semiconducting nanospheres. Advanced Materials 15 (10), pp. 800 - 804 (2003)

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Piok, T.; Romaner, L.; Gadermaier, C.; Wenzl, F. P.; Patil, S.; Montenegro, R.; Landfester, K.; Lanzani, G.; Cerullo, G.; Scherf, U. et al.; List, E. J. W.: A detailed study of the photophysics of organic semiconducting nanospheres. Synthetic Metals 139 (3), pp. 609 - 612 (2003)

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Pol, V. G.; Motiei, M.; Gedanken, A.; Calderon-Moreno, J.; Mastai, Y.: Sonochemical deposition of air-stable iron nanoparticles on monodispersed carbon spherules. Chemistry of Materials 15 (6), pp. 1378 - 1384 (2003)

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Ramirez, L. P.; Landfester, K.: Magnetic polystyrene nanoparticles with a high magnetite content obtained by miniemulsion processes. Macromolecular Chemistry and Physics 204 (1), pp. 22 - 31 (2003)

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Rana, R. K.; Zhang, L. Z.; Yu, J. C.; Mastai, Y.; Gedanken, A.: Mesoporous structures from supramolecular assembly of in situ generated ZnS nanoparticles. Langmuir 19 (14), pp. 5904 - 5911 (2003)

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Rharbi, Y.; Bechthold, N.; Landfester, K.; Salzman, A.; Winnik, M. A.: Solute exchange in synperonic surfactant micelles. Langmuir 19 (1), pp. 10 - 17 (2003)

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Rottstegge, J.; Kindervater, P.; Wilhelm, M.; Landfester, K.; Heldmann, C.; Fischer, J. P.; Spiess, H. W.: The influence of sodium ethene sulphonate comonomer on the film formation process of poly(vinyl acetate) dispersions. Colloid and Polymer Science 281 (12), pp. 1111 - 1120 (2003)

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Rottstegge, J.; Traub, B.; Wilhelm, M.; Landfester, K.; Heldmann, C.; Spiess, H. W.: Investigations on the film-formation process of latex dispersions by solid-state NMR spectroscopy. Macromolecular Chemistry and Physics 204 (5-6), pp. 787 - 802 (2003)

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Schlaad, H.; Antonietti, M.: Block copolymers with amino acid sequences: Molecular chimeras of polypeptides and synthetic polymers. European Physical Journal E 10 (1), pp. 17 - 23 (2003)

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Schlaad, H.; Kilz, P.: Determination of molecular weight distributions of diblock copolymers with conventional size exclusion chromatography. Analytical Chemistry 75 (6), pp. 1548 - 1551 (2003)

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Schrage, S.; Sigel, R.; Schlaad, H.: Formation of amphiphilic polyion complex vesicles from mixtures of oppositely charged block ionomers. Macromolecules 36 (5), pp. 1417 - 1420 (2003)

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Sedlak, M.; Hanusek, J.; Hejtmankova, L.; Kasparova, P.: Kinetics and mechanism of ring transformation of S-1-(4- methoxyphenyl)pyrrolidin-2-on-3-yl isothiuronium bromide to 2- methylimino-5-2-(4-methoxyphenylamino)ethyl thiazolidin-4-one. Organic & Biomolecular Chemistry 1 (7), pp. 1204 - 1209 (2003)

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Sedlak, M.; Simunek, P.; Antonietti, M.: Synthesis and N-15 NMR characterization of 4-vinylbenzyl substituted bases of nucleic acids. Journal of heterocyclic chemistry: the international journal of heterocyclic chemistry 40 (4), pp. 671 - 675 (2003)

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Shchukin, D. G.; Caruso, R. A.: Inorganic macroporous films from preformed nanoparticles and membrane templates: synthesis and investigation of photocatalytic and photoelectrochemical properties. Advanced Functional Materials 13 (10), pp. 789 - 794 (2003)

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Shchukin, D. G.; Caruso, R. A.: Template synthesis of porous gold microspheres. Chemical Communications (13), pp. 1478 - 1479 (2003)

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Shchukin, D. G.; Schattka, J. H.; Antonietti, M.; Caruso, R. A.: Photocatalytic properties of porous metal oxide networks formed by nanoparticle infiltration in a polymer gel template. The Journal of Physical Chemistry B 107 (4), pp. 952 - 957 (2003)

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Taden, A.; Antonietti, M.; Landfester, K.: Enzymatic polymerization towards biodegradable polyester nanoparticles. Macromolecular Rapid Communications 24 (8), pp. 512 - 516 (2003)

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Taden, A.; Landfester, K.: Crystallization of poly(ethylene oxide) confined in miniemulsion droplets. Macromolecules 36 (11), pp. 4037 - 4041 (2003)

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Tauer, K.; Ahmad, H.: Study on the preparation and stabilization of pyrene labeled polymer particles in nonpolar media. Polymer Reaction Engineering 11 (3), pp. 305 - 318 (2003)

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Tauer, K.; Müller, H.: On the role of initiator in emulsion polymerization. Colloid and Polymer Science 281 (1), pp. 52 - 65 (2003)

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Tauer, K.; Ramirez, A. G.; Lopez, R. G.: Effect of the surfactant concentration on the kinetics of oil in water microemulsion polymerization: a case study with butyl acrylate. Comptes Rendus Chimie 6, pp. 1245 - 1266 (2003)

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Tauer, K.; Yildiz, U.: Reactive poly(ethylene glycol)s in aqueous radical heterophase polymerization. Macromolecules 36 (23), pp. 8638 - 8647 (2003)

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Thomas, A.; Antonietti, M.: Silica nanocasting of simple cellulose derivatives: towards chiral pore systems with long-range order and chiral optical coatings. Advanced Functional Materials 13 (10), pp. 763 - 766 (2003)

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Thomas, A.; Polarz, S.; Antonietti, M.: Influence of spatial restrictions on equilibrium reactions: a case study about the excimer formation of pyrene. The Journal of Physical Chemistry B 107 (21), pp. 5081 - 5087 (2003)

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Thomas, A.; Schlaad, H.; Smarsly, B.; Antonietti, M.: Replication of lyotropic block copolymer mesophases into porous silica by nanocasting: learning about finer details of polymer self-assembly. Langmuir 19 (10), pp. 4455 - 4459 (2003)

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Viala, S.; Antonietti, M.; Tauer, K.; Bremser, W.: Structural control in radical polymerization with 1,1 diphenylethylene: 2. Behavior of MMA-DPE copolymer in radical polymerization. Polymer 44 (5), pp. 1339 - 1351 (2003)

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Voigt, U.; Khrenov, V.; Tauer, K.; Hahn, M.; Jaeger, W.; Klitzing, R. v.: The effect of polymer charge density and charge distribution on the formation of multilayers. Journal of Physics: Condensed Matter 15 (1), pp. S213 - S218 (2003)

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Journal Article (2457)